Semivolatile Organics US EPA Method 8270 on Rtx-5Sil MS

Peaks
1.N-Nitrosodimethylamine
2.Pyridine
3.Methyl methanesulfonate
4.2-Fluorophenol
5.Ethyl methanesulfonate
6.Phenol-d6-
7.Phenol
8.Aniline
9.bis(2-chloroethyl)ether
10.2-chlorophenol-d4
11.2-Chlorophenol
12.1,3-Dichlorobenzene
13.1,4-Dichlorobenzene-D4
14.1,4-Dichlorobenzene
15.Benzyl Alcohol
16.1,2-Dichlorobenzene-D4
17.1,2-Dichlorobenzene
18.2-Methylphenol
19.Bis(2-Chloroisopropyl)ether
20.4-Methylphenol/3-Methylphenol
21.N-Nitrosodipropylamine
22.Acetophenone
23.Hexachloroethane
24.Nitrobenzene-D5
25.Nitrobenzene
26.Isophorone
27.2,4-Dimethylphenol
28.2-Nitrophenol
29.Benzoic acid
30.Bis(2-chloroethoxy)methane
31.2,4-Dichlorophenol
32.1,2,4-Trichlorobenzene
33.Naphthalene-D8
34.Naphthalene
35.2,6-Dichlorophenol
36.4-Chloroaniline
37.Hexachloropropene
38.Hexachlorobutadiene
39.4-Chloro-3-methylphenol
40.Isosafrole
41.2-Methylnaphthalene
42.1-Methylnaphthalene
43.Hexachlorocyclopentadiene
44.1,2,4,5-Tetrachlorobenzene
45.2,4,6-Trichlorophenol
46.2,4,5-Trichlorophenol
47.2-Fluorobiphenyl
48.Safrole
49.2-Chloronaphthalene
50.2-Nitroaniline
51.1,4-Naphthoquinone
52.Dimethyl phthalate
53.1,3-Dinitrobenzene
Peaks
54.2,6-Dinitrotoluene
55.Acenaphthylene
56.3-Nitroaniline
57.Acenaphthene-d10
58.Acenaphthene
59.2,4-Dinitrophenol
60.4-Nitrophenol
61.Pentachlorobenzene
62.2,4-Dinitrotoluene
63.Dibenzofuran
64.2,3,4,6-Tetrachlorophenol
65.Diethyl Phthalate
66.4-Chlorophenyl phenyl ether
67.Fluorene
68.4-Nitroaniline
69.4,6-Dinitro-2-methylphenol
70.Diphenylamine
71.Azobenzene
72.2,4,6-Tribromophenol
73.Phenacetin
74.4-Bromophenyl phenyl ether
75.Hexachlorobenzene
76.Pentachlorophenol
77.Pentachloronitrobenzene
78.Dinoseb
79.Phenanthrene-D10
80.Phenanthrene
81.Anthracene
82.di-n-Butyl phthalate
83.4-nitroquinoline-1-oxide
84.Isodrin
85.Fluoranthene
86.Benzidine
87.Pyrene
88.Aramite
89.p-Terphenyl-d14
90.Chlorbenzilate
91.Benzyl butyl phthalate
92.Kepone
93.Bis(2-ethylhexyl)phthalate
94.3,3'-Dichlorobenzidine
95.Benzo[a]anthracene
96.Chrysene-D12
97.Chrysene
98.Di-n-octyl phthalate
99.Benzo[b]fluoranthene
100.Benzo[k]fluoranthene
101.Benzo[a]pyrene
102.Perylene-D12
103.3-Methylcholanthrene
104.Indeno[1,2,3-cd]pyrene
105.Dibenzo[a,h]anthracene
106.Benzo[ghi]perylene
image
GC_EV00532
ColumnRtx-5Sil MS, 30 m, 0.25 mm ID, 0.50 µm (cat.# 12738)
Sample8270 standard
Conc.:80 ng
Injectionsplitless
Inj. Temp.:300 °C
Oven
Oven Temp.:40 °C (hold 2 min) to 290 °C at 20 °C/min to 303 °C at 2 °C/min to 330 °C at 6 °C/min (hold 1 min)
Carrier GasHe, constant flow
Flow Rate:1.0 mL/min
DetectorMS
Mode:Scan
Source Temp.:280 °C
Scan Range:35-550 amu
InstrumentAgilent/HP6890 GC
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